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1. 新疆师范大学 物理系,新疆 乌鲁木齐,830054
2. 新疆师范大学 矿物发光及其微结构重点实验室,新疆 乌鲁木齐,830054
3. 新疆师范大学 理论物理自治区重点学科,新疆 乌鲁木齐,830054
纸质出版日期:2016-1-10,
收稿日期:2015-9-11,
修回日期:2015-11-16,
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庹娟, 王林香, 李敏. Li<sup>+</sup>、Na<sup>+</sup>和Eu<sup>3+</sup>共掺Lu<sub>2</sub>O<sub>3</sub>的制备及发光特性研究[J]. 发光学报, 2016,37(1): 28-32
TUO Juan, WANG Lin-xiang, LI Min. Preparation and Luminescence Properties of Li<sup>+</sup>, Na<sup>+</sup> and Eu<sup>3+</sup> Co-doped Lu<sub>2</sub>O<sub>3</sub>[J]. Chinese Journal of Luminescence, 2016,37(1): 28-32
庹娟, 王林香, 李敏. Li<sup>+</sup>、Na<sup>+</sup>和Eu<sup>3+</sup>共掺Lu<sub>2</sub>O<sub>3</sub>的制备及发光特性研究[J]. 发光学报, 2016,37(1): 28-32 DOI: 10.3788/fgxb20163701.0028.
TUO Juan, WANG Lin-xiang, LI Min. Preparation and Luminescence Properties of Li<sup>+</sup>, Na<sup>+</sup> and Eu<sup>3+</sup> Co-doped Lu<sub>2</sub>O<sub>3</sub>[J]. Chinese Journal of Luminescence, 2016,37(1): 28-32 DOI: 10.3788/fgxb20163701.0028.
用高温固相法合成了不同掺杂浓度的Li
+
、Na
+
和Eu
3+
共掺Lu
2
O
3
闪烁体发光材料
使用XRD进行结构表征
用扫描电镜观察了样品形貌
测量了激发光谱、发射光谱
分析了Li
+
、Na
+
和Eu
3+
的掺杂浓度以及温度对合成样品发光强度的影响。结果显示
Li
+
、Na
+
掺杂摩尔分数分别为2.5%和1%
在800 ℃空气中煅烧2 h制备的Lu
2
O
3
:5%Eu
3+
样品的发光最强。在同样条件下
比单掺2.5%Na
+
的样品发光强度提高1.89倍
比单掺2.5%Li
+
的样品发光强度提高3.97倍
比不掺Li
+
和Na
+
的样品发光强度提高6.43倍。
Li
+
Na
+
and Eu
3+
co-doped Lu
2
O
3
phosphors were synthesized by the high temperature solid-state reaction. The structure of the sample was characterized by XRD
the morphology was observed with scanning electron microscope
the excitation spectra and emission spectra were measured
and the effects of Li
+
Na
+
and Eu
3+
doping
concentration and the calcined temperature on the luminescence intensity of the synthesized samples were analyzed. The results show that the emission of the sample with 2.5%Li
+
1%Na
+
and 5%Eu
3+
co-doped Lu
2
O
3
is the strongest in the four samples calcined at 800 ℃ in the air for 2 h. In the same condition
the luminous intensity of Lu
2
O
3
:5%Eu
3+
2.5%Li
+
1%Na
+
is 1.89 times than that only with 2.5%Na
+
doping
3.97 times than that only with 2.5%Li
+
doping
and 6.43 times than that without Li
+
and Na
+
doping.
闪烁体Li+、Na+和Eu3+共掺Lu2O3高温固相法发光强度
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