Ni/SnO2复合薄膜的制备与光电性能

何瑞英; 魏长平; 王国栋; 伞靖; 彭春佳

doi:10.3788/fgxb20153608.0888

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Ni/SnO₂复合薄膜的制备与光电性能

材料合成及性能 | 更新时间：2020-08-12

- Ni/SnO₂复合薄膜的制备与光电性能
- Preparation and Photoelectric Properties of Ni/SnO₂ Composite Thin Films
- 发光学报 2015年36卷第8期页码：888-892
- 作者机构：
  
  长春理工大学化学与环境工程学院,吉林长春,130022
- 作者简介：
- 基金信息：
  
  吉林省教育厅"();十二五"();科学技术研究项目(吉教科合字[2013]第36号)资助()
- DOI：10.3788/fgxb20153608.0888
  中图分类号： O484.4;O614.43+2
- 纸质出版日期：2015-8-3，
  
  收稿日期：2015-5-19，
  
  修回日期：2015-6-12，
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何瑞英, 魏长平, 王国栋等. Ni/SnO2复合薄膜的制备与光电性能[J]. 发光学报, 2015,36(8): 888-892

HE Rui-ying, WEI Chang-ping, WANG Guo-dong etc. Preparation and Photoelectric Properties of Ni/SnO2 Composite Thin Films[J]. Chinese Journal of Luminescence, 2015,36(8): 888-892
何瑞英, 魏长平, 王国栋等. Ni/SnO2复合薄膜的制备与光电性能[J]. 发光学报, 2015,36(8): 888-892 DOI： 10.3788/fgxb20153608.0888.

HE Rui-ying, WEI Chang-ping, WANG Guo-dong etc. Preparation and Photoelectric Properties of Ni/SnO2 Composite Thin Films[J]. Chinese Journal of Luminescence, 2015,36(8): 888-892 DOI： 10.3788/fgxb20153608.0888.

摘要

采用旋涂法将溶胶-凝胶法制备的Ni/SnO

凝胶在玻璃基底上镀膜

得到了Ni/SnO

复合薄膜

探讨了镍掺杂量、煅烧温度对薄膜结构和形貌的影响.通过X射线衍射、红外光谱、扫描电子显微镜等测试手段对Ni/SnO

复合膜的结构和形貌进行表征.结果显示

500 ℃ 下煅烧的薄膜样品的结晶度较高

粒径小

颗粒分布均匀.用紫外-可见分光光度计和四探针电阻仪对其进行光学、电学性能测试

结果显示:适量的Ni掺杂可以提高SnO

薄膜在近紫外光区的吸收

Ni/SnO

薄膜在近紫外光区的吸收随着Ni

掺杂摩尔分数从5%增加到10%而逐渐减小.当Ni

掺杂摩尔分数为6%时

Ni/SnO

复合薄膜的导电性能最好.

Abstract

Ni/SnO

films were prepared by spin coating Ni/SnO

gel on the glass substrates. The effects of the doping amount of nickel and calcination temperature on the structure and morphology of Ni/SnO

films were discussed. The structure and morphology of Ni/SnO

composite film were characterized by using XRD

SEM and other testing methods. The results show that the particles of the film calcined at 500 ℃ have high crystallization

small size

and distribute uniformly. The right amount of Ni

doping can improve the absorbance in the near ultraviolet region of SnO

film

and the absorbance in the near ultraviolet region of Ni/SnO

film decreases with the increasing of Ni

mole fraction from 5% to 10%. The conductivity of Ni/SnO

film is the best when Ni

mole fraction is 6%.

关键词

Ni/SnO2复合薄膜溶胶-凝胶功能材料

Keywords

Ni/SnO2composite thin filmssol-gelfunctional materials

references

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Jia R J, Peng T J, Sun H J, et al. Preparation and characterization of rutile Ni-doped SnO2 nanoparticles [J]. Fine Chemicals (精细化工), 2008, 25(1):23-27 (in Chinese).

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