Dy³⁺和Ce³⁺共掺Y₃Al₅O₁₂荧光粉的制备及发光性质

{ "defaultlang": "zh", "titlegroup": { "articletitle": [ { "lang": "zh", "data": [ { "name": "text", "data": "Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "和Ce" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "共掺Y" }, { "name": "sub", "data": [ { "name": "text", "data": "3" } ] }, { "name": "text", "data": "Al" }, { "name": "sub", "data": [ { "name": "text", "data": "5" } ] }, { "name": "text", "data": "O" }, { "name": "sub", "data": [ { "name": "text", "data": "12" } ] }, { "name": "text", "data": "荧光粉的制备及发光性质" } ] }, { "lang": "en", "data": [ { "name": "text", "data": "Luminescent Properties of Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": ", Ce" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": " Co-doped Y" }, { "name": "sub", "data": [ { "name": "text", "data": "3" } ] }, { "name": "text", "data": "Al" }, { "name": "sub", "data": [ { "name": "text", "data": "5" } ] }, { "name": "text", "data": "O" }, { "name": "sub", "data": [ { "name": "text", "data": "12" } ] }, { "name": "text", "data": " Phosphors" } ] } ] }, "contribgroup": { "author": [ { "name": [], "stringName": [ { "lang": "zh", "surname": "王林香", "prefix": "" }, { "lang": "en", "surname": "WANG Lin-xiang", "prefix": "" } ], "aff": [ { "rid": "1665717", "text": "1" }, { "rid": "1826265", "text": "3" } ], "role": [ "first-author" ], "deceased": false }, { "name": [], "stringName": [ { "lang": "zh", "surname": "孙德方", "prefix": "" }, { "lang": "en", "surname": "SUN De-fang", "prefix": "" } ], "aff": [ { "rid": "1823961", "text": "2" } ], "role": [], "deceased": false }, { "name": [], "stringName": [ { "lang": "zh", "surname": "李晴", "prefix": "" }, { "lang": "en", "surname": "LI Qing", "prefix": "" } ], "aff": [ { "rid": "1665717", "text": "1" }, { "rid": "1826265", "text": "3" } ], "role": [], "deceased": false }, { "name": [], "stringName": [ { "lang": "zh", "surname": "王霞", "prefix": "" }, { "lang": "en", "surname": "WANG Xia", "prefix": "" } ], "aff": [ { "rid": "1665717", "text": "1" } ], "role": [], "deceased": false } ], "aff": [ { "id": "1665717", "intro": [ { "lang": "zh", "label": "1", "text": " 新疆师范大学 物理与电子工程学院,新疆 乌鲁木齐,830054", "data": [ { "name": "text", "data": " 新疆师范大学 物理与电子工程学院,新疆 乌鲁木齐,830054" } ] }, { "lang": "en", "label": "1", "text": " College of Physics and Electronic Engineering, Xinjiang Normal University", "data": [ { "name": "text", "data": " College of Physics and Electronic Engineering, Xinjiang Normal University" } ] } ] }, { "id": "1823961", "intro": [ { "lang": "zh", "label": "2", "text": " 新疆师范高等专科学校(新疆教育学院), 新疆 乌鲁木齐 830043", "data": [ { "name": "text", "data": " 新疆师范高等专科学校(新疆教育学院), 新疆 乌鲁木齐 830043" } ] }, { "lang": "en", "label": "2", "text": " School of Mathematics, Xinjiang Teacher's College(Xinjiang Education Institute), Urumqi 830043, China", "data": [ { "name": "text", "data": " School of Mathematics, Xinjiang Teacher's College(Xinjiang Education Institute), Urumqi 830043, China" } ] } ] }, { "id": "1826265", "intro": [ { "lang": "zh", "label": "3", "text": " 新疆师范大学 矿物发光及其微结构重点实验室,新疆 乌鲁木齐,830054", "data": [ { "name": "text", "data": " 新疆师范大学 矿物发光及其微结构重点实验室,新疆 乌鲁木齐,830054" } ] }, { "lang": "en", "label": "3", "text": " Key Laboratory of Novel Luminescent Materials and Nanostructures, Xinjiang Normal University, Urumqi 830054, China", "data": [ { "name": "text", "data": " Key Laboratory of Novel Luminescent Materials and Nanostructures, Xinjiang Normal University, Urumqi 830054, China" } ] } ] } ] }, "abstracts": [ { "lang": "zh", "data": [ { "name": "p", "data": [ { "name": "text", "data": "用高温固相法制备了YAG:5% Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "以及（Ce" }, { "name": "sub", "data": [ { "name": "text", "data": "0.01" } ] }, { "name": "text", "data": "Dy" }, { "name": "sub", "data": [ { "name": "text", "data": "y" } ] }, { "name": "text", "data": "Y" }, { "name": "sub", "data": [ { "name": "text", "data": "0.99-" }, { "name": "text", "data": "y" } ] }, { "name": "text", "data": "）" }, { "name": "sub", "data": [ { "name": "text", "data": "3" } ] }, { "name": "text", "data": "A1" }, { "name": "sub", "data": [ { "name": "text", "data": "5" } ] }, { "name": "text", "data": "O" }, { "name": "sub", "data": [ { "name": "text", "data": "12" } ] }, { "name": "text", "data": "（" }, { "name": "text", "data": "y" }, { "name": "text", "data": "=0%，1%，3%，5%，7%，9%）荧光粉。XRD结果表明，NH" }, { "name": "sub", "data": [ { "name": "text", "data": "4" } ] }, { "name": "text", "data": "Cl、LiCl、H" }, { "name": "sub", "data": [ { "name": "text", "data": "3" } ] }, { "name": "text", "data": "BO" }, { "name": "sub", "data": [ { "name": "text", "data": "3" } ] }, { "name": "text", "data": "三种助熔剂比较，添加H" }, { "name": "sub", "data": [ { "name": "text", "data": "3" } ] }, { "name": "text", "data": "BO" }, { "name": "sub", "data": [ { "name": "text", "data": "3" } ] }, { "name": "text", "data": "可有效降低YAG晶体的结晶温度，有效阻止中间相YAlO" }, { "name": "sub", "data": [ { "name": "text", "data": "3" } ] }, { "name": "text", "data": "的形成。H" }, { "name": "sub", "data": [ { "name": "text", "data": "3" } ] }, { "name": "text", "data": "BO" }, { "name": "sub", "data": [ { "name": "text", "data": "3" } ] }, { "name": "text", "data": "做助熔剂在1 450℃煅烧6 h制备的Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "和Ce" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "掺杂Y" }, { "name": "sub", "data": [ { "name": "text", "data": "3" } ] }, { "name": "text", "data": "Al" }, { "name": "sub", "data": [ { "name": "text", "data": "5" } ] }, { "name": "text", "data": "O" }, { "name": "sub", "data": [ { "name": "text", "data": "12" } ] }, { "name": "text", "data": "荧光粉具有单一YAG立方相结构，且随Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "掺杂浓度增加，（420）衍射峰逐渐向小角度偏移。在583 nm监测下；与单掺1% Ce" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "样品比较，Ce" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "与Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "共掺样品在342 nm处的吸收均减弱；与单掺5% Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "样品比较，Ce" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "与Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "共掺样品在351 nm处的吸收明显增强。351 nm激发下，随Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "掺杂浓度增加，Ce" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "与Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "共掺样品中Ce" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "在526 nm处的发射强度逐渐减小，而在583 nm处的发射强度先增加后减弱，这说明351 nm激发下，Ce" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "与Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "共掺样品中存在Ce" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "向Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "的部分能量传递。465 nm激发下，Ce" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "与Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "共掺杂样品中只出现Ce" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "的发射峰，且随Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "浓度增加，Ce" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "发光减弱。当Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "离子浓度为3%时，Ce" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "与Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "共掺样品中Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "相对光强达到最大，此时Ce" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "能量传递效率为15.7%。405 nm激发下，随Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "掺杂浓度增加，合成粉体中Ce" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "的寿命逐渐减小。经计算，Ce" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "能量传递临界距离为3.464 nm，为电四极-电四极相互作用的共振能量传递。" } ] } ] }, { "lang": "en", "data": [ { "name": "p", "data": [ { "name": "text", "data": "YAG:5%Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": " and (Ce" }, { "name": "sub", "data": [ { "name": "text", "data": "0.01" } ] }, { "name": "text", "data": "Dy" }, { "name": "sub", "data": [ { "name": "text", "data": "y" } ] }, { "name": "text", "data": "Y" }, { "name": "sub", "data": [ { "name": "text", "data": "0.99-" }, { "name": "text", "data": "y" } ] }, { "name": "text", "data": ")" }, { "name": "sub", "data": [ { "name": "text", "data": "3" } ] }, { "name": "text", "data": "A1" }, { "name": "sub", "data": [ { "name": "text", "data": "5" } ] }, { "name": "text", "data": "O" }, { "name": "sub", "data": [ { "name": "text", "data": "12" } ] }, { "name": "text", "data": " (" }, { "name": "text", "data": "y" }, { "name": "text", "data": "=0%,1%,3%,5%,7%,9%) phosphors were prepared by high temperature solid-state method. XRD results showed that the addition of H" }, { "name": "sub", "data": [ { "name": "text", "data": "3" } ] }, { "name": "text", "data": "BO" }, { "name": "sub", "data": [ { "name": "text", "data": "3" } ] }, { "name": "text", "data": " could effectively reduce the crystallization temperature of YAG crystal and prevent the formation of the intermediate phase YAlO" }, { "name": "sub", "data": [ { "name": "text", "data": "3" } ] }, { "name": "text", "data": ". The results showed that they were still the cubic phase of the samples for Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": ", Ce" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": " doped Y" }, { "name": "sub", "data": [ { "name": "text", "data": "3" } ] }, { "name": "text", "data": "Al" }, { "name": "sub", "data": [ { "name": "text", "data": "5" } ] }, { "name": "text", "data": "O" }, { "name": "sub", "data": [ { "name": "text", "data": "12" } ] }, { "name": "text", "data": " by adding H" }, { "name": "sub", "data": [ { "name": "text", "data": "3" } ] }, { "name": "text", "data": "BO" }, { "name": "sub", "data": [ { "name": "text", "data": "3" } ] }, { "name": "text", "data": " after calcination at 1 450℃ for 6 h. With the increase of Dy " }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": " doping concentration, the main diffraction peak (420) shifted to a small angle. Under " }, { "name": "text", "data": "" }, { "name": "sub", "data": [ { "name": "text", "data": "em" } ] }, { "name": "text", "data": "=583 nm, the absorptions of Ce" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": " and Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": " co-doped samples at 342 nm were decreased than that of only Ce" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": " doped sample, and the absorptions at 351 nm significantly enhanced compared with that of only Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": " doped sample. Under 351 nm excitation, with the increase of Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": " doping concentration, the emission intensities at 526 nm decreased for Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": " and Ce" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": " co-doped Y" }, { "name": "sub", "data": [ { "name": "text", "data": "3" } ] }, { "name": "text", "data": "Al" }, { "name": "sub", "data": [ { "name": "text", "data": "5" } ] }, { "name": "text", "data": "O" }, { "name": "sub", "data": [ { "name": "text", "data": "12" } ] }, { "name": "text", "data": " samples, but the emission intensities at 583 nm first increased and then decreased, which indicated that under the excitation of 351 nm, part of the energy transfer from Ce" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": " to Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": " existed. Under 465 nm excitation, Ce" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": " and Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": " co-doped samples only contained Ce" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": " emission peak, and with the increase of Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": " concentration, emissions of Ce" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": " ions decreased. When the concentration of Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": " was 3%, the emission intensity of Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": " reached the maximum, and the energy transfer efficiency of Ce" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": " was 15.7%. Under 405 nm excitation, with the increase of Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": " concentration, the lifetime of Ce" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": " decreased for Ce" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": " and Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": " co-doped samples. The critical distance of Ce" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": " energy transfer was 3.464 nm, which was the resonance energy transfer of the electric quadrupole-electric quadrupole interaction." } ] } ] } ], "keyword": [ { "lang": "zh", "data": [ [ { "name": "text", "data": "Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "和Ce" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": "共掺Y" }, { "name": "sub", "data": [ { "name": "text", "data": "3" } ] }, { "name": "text", "data": "Al" }, { "name": "sub", "data": [ { "name": "text", "data": "5" } ] }, { "name": "text", "data": "O" }, { "name": "sub", "data": [ { "name": "text", "data": "12" } ] } ], [ { "name": "text", "data": "发光性质" } ], [ { "name": "text", "data": "能量传递" } ], [ { "name": "text", "data": "能级寿命" } ], [ { "name": "text", "data": "多极相互作用" } ] ] }, { "lang": "en", "data": [ [ { "name": "text", "data": "Dy" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": " and Ce" }, { "name": "sup", "data": [ { "name": "text", "data": "3+" } ] }, { "name": "text", "data": " co-doped Y" }, { "name": "sub", "data": [ { "name": "text", "data": "3" } ] }, { "name": "text", "data": "Al" }, { "name": "sub", "data": [ { "name": "text", "data": "5" } ] }, { "name": "text", "data": "O" }, { "name": "sub", "data": [ { "name": "text", "data": "12" } ] } ], [ { "name": "text", "data": "luminescence properties" } ], [ { "name": "text", "data": "energy transfer" } ], [ { "name": "text", "data": "energy level lifetime" } ], [ { "name": "text", "data": "multipolar interaction" } ] ] } ], "highlights": [], "body": [], "footnote": [], "reflist": { "data": [ { "id": "ref1", "label": "1", "citation": [ { "lang": "zh", "text": [ { "name": "text", "data": "SCHUBERT E F,KIM J K. 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Front., 2018,5(5):1076-1084." } ] } ] } ] }, "response": [], "contributions": [], "acknowledgements": [], "conflict": [], "supportedby": [], "articlemeta": { "doi": "10.3788/fgxb20204102.0160", "clc": [ [ { "name": "text", "data": "O611.4;O482.31" } ] ], "dc": [], "citeme": [], "fundinggroup": [ { "lang": "zh", "text": [ { "name": "text", "data": "新疆维吾尔自治区自然科学基金（2017D01A60）资助项目" } ] }, { "lang": "en", "text": [ { "name": "text", "data": "Supported by Natural Science Foundation of Xinjiang(2017D01A60)" } ] } ], "history": { "received": "2019-10-07", "revised": "2019-10-23", "epub": "2019-11-19", "ppub": "2020-02-05", "opub": "2020-08-11" } }, "appendix": [], "ethics": [], "supplementary": [], "issue": "2", "volume": "41", "originalSource": [] }