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中国计量学院 材料科学与工程学院,浙江 杭州,310018
收稿日期:2014-02-28,
修回日期:2014-04-04,
纸质出版日期:2014-06-03
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王莉, 吕婷, 阮枫萍等. 水热法制备的荧光碳量子点[J]. 发光学报, 2014,35(6): 706-709
WANG Li, LYU Ting, RUAN Feng-ping etc. Synthesis of Photoluminescent Carbon Nanoparticles by Hydrothermal Method[J]. Chinese Journal of Luminescence, 2014,35(6): 706-709
王莉, 吕婷, 阮枫萍等. 水热法制备的荧光碳量子点[J]. 发光学报, 2014,35(6): 706-709 DOI: 10.3788/fgxb20143506.0706.
WANG Li, LYU Ting, RUAN Feng-ping etc. Synthesis of Photoluminescent Carbon Nanoparticles by Hydrothermal Method[J]. Chinese Journal of Luminescence, 2014,35(6): 706-709 DOI: 10.3788/fgxb20143506.0706.
以葡萄糖为碳源,通过水热法制备了碳量子点,并通过X射线衍射(XRD)、透射电镜(TEM)、紫外-可见吸收光谱、荧光光谱和傅里叶红外光谱(FTIR)等方法对样品的结构、形貌和光学性能进行表征。结果显示:以葡萄糖为碳源制备的碳量子点近似球形,大小均匀,分散性良好,无团聚现象。其发射波长依赖于激发波长,在紫外灯下发出明亮的绿光。
Carbon nanoparticles were synthesized
via
hydrothermal oxidation of glucose. The carbon dots were characterized by X-ray diffraction (XRD)
transmission electron microscopy (TEM)
ultraviolet-visible spectrophotometry
fluorescene spectrophotometry and Fourier transform infrared spectrophoto-metry (FTIR). The results indicate that the carbon dots have appropriate spherical morphology
uniform size
good dispersion
non-agglomeration. The carbon dots can emit bright green photoluminescence under UV excitation
and exhibit excitation-dependent PL behavior.
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