六角锥状ZnO纳米结构的生长机理、结构及光学性能

李东明; 李金华; 方 铉; 王晓华; 魏志鹏; 聂燕萍; 李春萍

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六角锥状ZnO纳米结构的生长机理、结构及光学性能

论文 | 更新时间：2020-08-12

- 六角锥状ZnO纳米结构的生长机理、结构及光学性能
- Growth Mechanism, Structural and Optical Properties of Hexagonal Cone-shaped ZnO Nanostructure
- 发光学报 2010年31卷第1期页码：114-118
- 作者机构：
  
  1. 长春理工大学理学院,吉林长春,130022
  2. 空军航空大学, 吉林长春 130022
- 作者简介：
- 基金信息：
- DOI：
  中图分类号： O482.31
- 收稿日期：2009-10-08，
  
  修回日期：1900-01-02，
  
  网络出版日期：2010-02-20，
  
  纸质出版日期：2010-02-20
- 稿件说明：
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李东明, 李金华, 方铉, 等. 六角锥状ZnO纳米结构的生长机理、结构及光学性能[J]. 发光学报, 2010,31(1):114-118.

LI Dong-ming, LI Jin-hua, FANG Xuan, et al. Growth Mechanism, Structural and Optical Properties of Hexagonal Cone-shaped ZnO Nanostructure[J]. Chinese journal of luminescence, 2010, 31(1): 114-118.
李东明, 李金华, 方铉, 等. 六角锥状ZnO纳米结构的生长机理、结构及光学性能[J]. 发光学报, 2010,31(1):114-118. DOI：

LI Dong-ming, LI Jin-hua, FANG Xuan, et al. Growth Mechanism, Structural and Optical Properties of Hexagonal Cone-shaped ZnO Nanostructure[J]. Chinese journal of luminescence, 2010, 31(1): 114-118. DOI：

摘要

利用醋酸锌和六次甲基四胺(C

)以一定比例配置成反应溶液

通过水热合成法制备了六角锥状ZnO纳米结构。同时

使用了扫描电子显微镜(SEM)、X射线衍射和选区电子衍射(SAED)

对样品的形貌与结构进行了分析。结果表明

样品形貌成六角锥状结构

并且在[002]方向择优生长。通过对样品的光学性能测试

由PL光谱分析可知

样品在379 nm处有一个较强的紫外发光峰

并且在可见光区域产生了一些较弱的可见光发射峰

表明制备的六角锥状ZnO纳米结构的晶体质量不是很好。除此之外

对六角锥状ZnO的生长机理也进行了讨论。

Abstract

Using a hydrothermal method

the single-crystalline ZnO nanowires with a hexagonal cone-shape were synthesized with zinc acetate and hexamethylenetetramine(HMT). The morphology of the hexagonal cone-shaped ZnO was investigated by selected area electron diffraction (SAED) and scanning electron microscopy (SEM) measurements. The photoluminescence (PL) spectrum of the synthesized ZnO nanowires shows a strong ultraviolet (UV) emission at 379 nm and some weak emission peaks at the visible wavelength region. In addition

the formation mechanism of the hexagonal cone-shaped ZnO is discussed.

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Keywords

references

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