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1. 中国科学院 研究生院 北京,100039
2. 发光学与应用国家重点实验室 中国科学院长春光学精密机械与物理研究所,吉林 长春,130033
纸质出版日期:2012-7-10,
网络出版日期:2012-7-10,
收稿日期:2012-3-28,
修回日期:2012-5-7,
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王新建, 宋航, 黎大兵, 蒋红, 李志明, 缪国庆, 陈一仁, 孙晓娟. 氮化铝薄膜的硅热扩散掺杂研究[J]. 发光学报, 2012,33(7): 768-773
WANG Xin-jian, SONG Hang, LI Da-bing, JIANG Hong, LI Zhi-ming, MIAO Guo-qing, CHEN Yi-ren, SUN Xiao-jun. Study of AlN Films Doped by Si Thermal Diffusion[J]. Chinese Journal of Luminescence, 2012,33(7): 768-773
王新建, 宋航, 黎大兵, 蒋红, 李志明, 缪国庆, 陈一仁, 孙晓娟. 氮化铝薄膜的硅热扩散掺杂研究[J]. 发光学报, 2012,33(7): 768-773 DOI: 10.3788/fgxb20123307.0768.
WANG Xin-jian, SONG Hang, LI Da-bing, JIANG Hong, LI Zhi-ming, MIAO Guo-qing, CHEN Yi-ren, SUN Xiao-jun. Study of AlN Films Doped by Si Thermal Diffusion[J]. Chinese Journal of Luminescence, 2012,33(7): 768-773 DOI: 10.3788/fgxb20123307.0768.
采用热扩散方法
对AlN薄膜进行了Si掺杂。利用电子能量散射谱(EDS)以及高温变温电导对薄膜进行了分析。EDS测试结果表明:在1 250 ℃的温度下
氮化硅(SiN
x
)作为Si的扩散源
可以实现对AlN薄膜的Si热扩散掺杂。高温电流-电压(I-V)测试表明:在460 ℃测试温度下
AlN薄膜在热扩散掺杂以后
其电导从1.9×10
-3
S·m
-1
增加到2.1×10
-2
S·m
-1
。高温变温电导测试表明:氮空位(V
3+
N
)和Si在AlN中的激活能为1.03 eV和0.45 eV。
This paper deals with the characteristics of aluminium nitride (AlN) films doped by silicon (Si) thermal diffusion. The films are analyzed by energy dispersive X-ray spectroscopy (EDS) and high-temperature dependent electrical conductivity. The results of EDS show that the Si element is successfully doped into the AlN films using SiN
x
as the diffusion source at the temperature of 1 250 ℃. The high-temperature current-voltage (I-V) measurements show that the electrical properties of the AlN films can be prominently improved by Si thermal diffusion
and at the measured temperature of 460 ℃ their electrical conductivities increase from 1.9×10
-3
S·m
-1
to 2.1×10
-2
S·m
-1
after the Si thermal diffusion. The high-temperature dependence of thermal conductivity suggests that the activation energies of V
3+
N
and Si are about 1.03 eV and 0.45 eV
respectively.
杂质氮化物热扩散
impuritiesnitridesthermal diffusion
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