亚微米级Ca2.40Lu0.54ScMgSi3O12：0.06Ce3+荧光粉的溶胶燃烧法合成与表征

陈旖勃; 潘英娇; 梁敏华; 冯静容

doi:10.3788/fgxb20143501.0073

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亚微米级Ca_2.40Lu_0.54ScMgSi₃O₁₂：0.06Ce³⁺荧光粉的溶胶燃烧法合成与表征

材料合成及性能 | 更新时间：2020-08-12

- 亚微米级Ca_2.40Lu_0.54ScMgSi₃O₁₂：0.06Ce³⁺荧光粉的溶胶燃烧法合成与表征
- Sol-combustion Synthesis and Analysis of Submicron Sized Ca_2.40Lu_0.54ScMgSi₃O₁₂：0.06Ce³⁺ Phosphor for White Light Emitting Diodes
- 发光学报 2014年35卷第1期页码：73-78
- 作者机构：
  
  广州大学化学化工学院,广东广州,510006
- 作者简介：
- 基金信息：
  
  国家自然科学基金（51102054）();广东省创新人才培育项目（LYM10107）();广州大学大学生创新训练项目（2013年01号）资助()
- DOI：10.3788/fgxb20143501.0073
  中图分类号： O482.31
- 收稿日期：2013-08-20，
  
  修回日期：2013-09-17，
  
  纸质出版日期：2014-01-03
- 稿件说明：
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陈旖勃, 潘英娇, 梁敏华, 冯静容. 亚微米级Ca2.40Lu0.54ScMgSi3O12：0.06Ce3+荧光粉的溶胶燃烧法合成与表征[J]. 发光学报, 2014,35(1): 73-78

CHEN Yi-bo, PAN Ying-jiao, LIANG Min-hua, FENG Jing-rong. Sol-combustion Synthesis and Analysis of Submicron Sized Ca2.40Lu0.54ScMgSi3O12：0.06Ce3+ Phosphor for White Light Emitting Diodes[J]. Chinese Journal of Luminescence, 2014,35(1): 73-78
陈旖勃, 潘英娇, 梁敏华, 冯静容. 亚微米级Ca2.40Lu0.54ScMgSi3O12：0.06Ce3+荧光粉的溶胶燃烧法合成与表征[J]. 发光学报, 2014,35(1): 73-78 DOI： 10.3788/fgxb20143501.0073.

CHEN Yi-bo, PAN Ying-jiao, LIANG Min-hua, FENG Jing-rong. Sol-combustion Synthesis and Analysis of Submicron Sized Ca2.40Lu0.54ScMgSi3O12：0.06Ce3+ Phosphor for White Light Emitting Diodes[J]. Chinese Journal of Luminescence, 2014,35(1): 73-78 DOI： 10.3788/fgxb20143501.0073.

摘要

用溶胶燃烧法在1 200 ℃制备了亚微米级Ca

2.40

0.54

ScMgSi

：0.06Ce

荧光粉，并对其进行了物相结构、形貌、光致发光性质和热猝灭性质的表征。与传统高温固相法制备的样品相比，溶胶燃烧法不但降低了制备温度，而且制备的Ca

2.40

0.54

ScMgSi

：0.06Ce

荧光粉的形貌也有所改善。发光性质测试结果表明，亚微米级Ca

2.40

0.54

ScMgSi

：0.06Ce

荧光粉的发光峰值相比于高温固相法样品有约10 nm的红移，而且样品的热猝灭性质也优于高温固相法样品。

Abstract

Submicron sized Ca

2.40

0.54

ScMgSi

:0.06Ce

phosphor was prepared by sol-combustion (SC) method. The phase-forming

morphology

photoluminescence and thermal quenching properties of phosphor were investigated. The results confirm that the Ca

2.40

0.54

ScMgSi

:0.06Ce

phosphor can be prepared by SC method at 1ower temperature

and the morphology is much more uniform than the samples prepared by solid state (SS) method. Photoluminescence measurements show that the emission of the submicron sized Ca

2.40

0.54

ScMgSi

:0.06Ce

phosphor presents a ~10 nm red shift compared with the SS sample

and the thermal quenching of the submicron sized Ca

2.40

0.54

ScMgSi

:0.06Ce

phosphor is obviously weaker.

关键词

Keywords

references

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