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1. 中国科学院 长春光学精密机械与物理研究所,吉林 长春,中国,130033
2. 中国科学院大学 北京,100049
收稿日期:2013-01-17,
修回日期:2013-03-02,
网络出版日期:2013-03-15,
纸质出版日期:2013-05-10
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陈少杰, 齐向东, 巴音贺希格, 唐玉国, 曹海霞. 用于激光诱导等离子体光谱分析的便携式中阶梯光栅光谱仪设计[J]. 发光学报, 2013,34(5): 672-677
CHEN Shao-Jie, JI Xiang-Dong, BA Yin-He-Xi-Ge, TANG Yu-Guo, CAO Hai-Xia. A Portable Echelle Spectrograph Design for Laser-induced Breakdown Spectroscopy[J]. Chinese Journal of Luminescence, 2013,34(5): 672-677
陈少杰, 齐向东, 巴音贺希格, 唐玉国, 曹海霞. 用于激光诱导等离子体光谱分析的便携式中阶梯光栅光谱仪设计[J]. 发光学报, 2013,34(5): 672-677 DOI: 10.3788/fgxb20133405.0672.
CHEN Shao-Jie, JI Xiang-Dong, BA Yin-He-Xi-Ge, TANG Yu-Guo, CAO Hai-Xia. A Portable Echelle Spectrograph Design for Laser-induced Breakdown Spectroscopy[J]. Chinese Journal of Luminescence, 2013,34(5): 672-677 DOI: 10.3788/fgxb20133405.0672.
激光诱导等离子体光谱分析技术是一种非接触式实时检测技术
它已成为一种新兴的物质成分与浓度分析手段
并在工业生产等领域有着重要应用。为了使激光诱导等离子体光谱分析技术在极短的时间内同时获得全面的光谱信息
本文设计了一款波段范围为180~400 nm的轻小型中阶梯光栅光谱仪。通过分析其光学性能
确定了系统的结构参数
并对像差进行了分析校正。对汞灯特征光谱进行了测试标定
仪器光谱分辨率在253.652 nm处可达0.036 8 nm
满足激光诱导光谱分析技术对仪器光学性能的需求。
Laser-induced breakdown spectroscopy (LIBS) has attracted increasing interest and is widely used for routine elemental analysis. In order to enable LIBS to detect complete spectral information within a quite short time
a small size echelle spectrograph with spectral coverage from 180~400 nm was designed. According to the analysis of the optical system
the parameters are calculated and the aberrations are corrected well. In this way
this echelle spectrograph can obtain two-dimension spectral graph with high resolution quickly. By testing and calibrating the Hg lamp
the actual resolution gets up to 0.036 8 nm at 253.652 nm which can satisfy the analysis requirement of LIBS.
Walid Tawfik Y Mohamed. Improved LIBS limit of detection of Be, Mg, Si, Mn, Fe and Cu in aluminum alloy samples using a portable Echelle spectrometer with ICCD camera [J]. Optics & Laser Technology, 2008, 40(1):30-38.[2] Leon J Radziemski. From LASER to LIBS, the path of technology development [J]. Spectrochimica Acta Part B, 2002, 57(7):1109-1113.[3] Ahmed R, Baig M. On the Optimization for enhanced dual-pulse laser-induced breakdown sectroscopy [J]. IEEE Transactins on Plasma Science, 2010, 38(8):2052-2055.[4] Tao M M,Yang P L, Liu W P, et al. Response characteristics of fiber Bragg gratings irradiated by high energy lasers [J]. Chin. Opt.(中国光学), 2012, (5):544-549.[5] Ye J F, Hong Y J, Wang G Y, et al. Research progress in micro-laser plasma propulsion [J]. Chin. Opt.(中国光学), 2011, 4(4):319-326 (in Chinese).[6] Noll R, Bette H, Brysch A, et al. Laser-induced breakdown spectrometry -applications for production control and quality assurance in the steel industry [J]. Spectromchimica Acta Part B, 2001, 56:637-649.[7] Stankova A, Gilon N, Dutruch L, et al. A simple LIBS method for fast quantitative analysis of fly ashes [J]. Fuel, 2010, 89(11):3468-3474.[8] Huang Q. The Emission studies on ultraviolet laser ablation of copper in low pressure [J]. Chin. J. Lumin.(发光学报), 2006, 27(6):1021-1025 (in Chinese).[9] Hu J, Chen G, Zen Y. Studies on laser-induced filuorimetry(IX) the luminescence mechanism and analytical application of Dy-AA-TOPO-SLS fluorescent system [J]. Chin. J. Lumin. (发光学报), 1991, 12(1):66-72 (in Chinese).[10] Bauer H, Leis F, Niemax K. Laser induced breakdown spectrometry with an echelle spectrometer and intensified chage coupled device detection [J]. Spectrochimica Acta Part B,1998, 53(12):1815-1825.[11] Haisch C, Panne U, Niessner R. Combination of an intensified charge coupled device with an echelle spectrograph for analysis of colloidal material by laser-induced plasma spectroscopy [J]. Spectrochimica Acta Part B,1998, 53:1657-1667.[12] Florek S, Haisch C, Okruss M, et al. H. A new, versatile echelle spectrometer relevant to laser induced plasma applications [J]. Spectrochimica Acta Part B, 2001, 56(6):1027-1034.[13] Lindblom P. New compact echelle spectrographs with multichannel time-resolved recording capabilities [J]. Analytica Chimica Acta, 1999, 380(2/3):353-361.[14] Wu N, Tan X, Bayanheshig, Tang Y G, et al. Simulation and experiments of ion beam etching process for blazed holographic grating [J]. Opt. Precision Eng.(光学 精密工程), 2012, 20(9):1904-1912 (in Chinese).[15] Tang Y G, He M, Cui J C, et al. Senamont based measuring method for birefringence of infrared crystal [J]. Opt. Precision Eng.(光学 精密工程), 2012, 20(10): 2176-2183 (in Chinese).[16] Tang Y, Chen H, Zhang Z, et al. Multi-Channel Spectrometer based on Linear CCD and its Application [J]. Huazhong Univ. of Sci. & Tech.(华中科技大学学报), 2002, 30(10):96-98 (in Chinese).
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