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长春理工大学 理学院,吉林 长春,130022
收稿:2009-05-11,
修回:1900-1-2,
网络出版:2009-12-30,
纸质出版:2009-12-30
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姜德龙, 王 新, 向 嵘, 等. 磁控溅射制备氧化硅薄膜生长速率[J]. 发光学报, 2009,30(6):888-891.
JIANG De-long, WANG Xin, XIANG Rong, et al. Deposition Rate of Thin Silicon Oxide Film by Magnetron Sputtering Method[J]. Chinese Journal of Luminescence, 2009, 30(6): 888-891.
氧化硅薄膜是半导体工业中常见的薄膜材料
通常采用化学气相沉积方法制备。但是这种制备方法存在缺欠。采用磁控溅射的方法首先在石英衬底上制备了氧化硅薄膜。研究了射频功率、氧气含量和溅射压强对氧化硅薄膜沉积速率的影响。发现沉积速率随着射频功率的增加而增加;随着氧气含量的增加
先减小后增大;当溅射压强在0.4~0.8 Pa之间变化时
沉积速率变化很小
当溅射压强超过0.8 Pa时沉积速率迅速下降。讨论了不同生长条件下造成氧化硅薄膜生长速率变化的原因。
Silicon oxide is one of the thin films well known in semiconductor industry. It is commonly obtained by chemical vapor deposition (CVD). For this deposition technique
the great disadvantages are high temperature and dangerous reactants as silane (SiH
4
)
dichlo-rosilane (SiH
2
Cl
2
)
ammonia (NH
3
). The reactive magnetron sputtering is a powerful technique for deposition of many different types of films at low deposition temperature. Some of organic (carbon)
metallic (tungsten
aluminum
nickel
cobalt
etc.
)
semiconductor (silicon) and thin dielectric (aluminum oxide) films can commonly be obtained by this method
and furthermore
the advantage is utilization of non-toxic gases
for example
argon
oxygen and nitrogen
high-purity target (99.99%) and it is possible to obtain high deposition rate. In this paper
the silicon oxide films were deposited on quartz substrate by radio-frequency (RF) reactive magnetron sputtering method
the influences of radio-frequency power
oxygen concentration and sputtering pressure on the deposition rate of the silicon oxide film was investigated. It was found that the deposition rate increases with increasing the RF power
but firstly increases and then decreases with increasing oxygen concentration. The deposition rate changed little when the sputtering pressure changed in 0.4~0.8 Pa
and decreases drastically if the pressure is beyond 0.8 Pa. Finally
it was detailedly discused why the deposition rate of silicon oxide films at different growth condition changes.
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. Zamboma L S, Mansano R D, Mousinho A P. Low-temperature deposition of silicon oxide and silicon nitride by reactive magnetron sputtering [J]. Microelectronics Journal, 2009, 40 (1):66-69.
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