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天津工业大学 理学院 天津,300160
Received:22 March 2018,
Revised:24 July 2018,
Published Online:06 July 2018,
Published:05 January 2019
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魏利娟, 张海明, 曹静等. 静电纺Ag/WO<sub>3</sub>复合纳米纤维及其光催化性能[J]. 发光学报, 2019,40(1): 39-44
WEI Li-juan, ZHANG Hai-ming, CAO Jing etc. Electrospinning Fabrication of Ag/WO<sub>3</sub> Nanofibers and Photocatalytic Performance[J]. Chinese Journal of Luminescence, 2019,40(1): 39-44
魏利娟, 张海明, 曹静等. 静电纺Ag/WO<sub>3</sub>复合纳米纤维及其光催化性能[J]. 发光学报, 2019,40(1): 39-44 DOI: 10.3788/fgxb20194001.0039.
WEI Li-juan, ZHANG Hai-ming, CAO Jing etc. Electrospinning Fabrication of Ag/WO<sub>3</sub> Nanofibers and Photocatalytic Performance[J]. Chinese Journal of Luminescence, 2019,40(1): 39-44 DOI: 10.3788/fgxb20194001.0039.
为了研究氧化钨(WO
3
)和银/氧化钨(Ag/WO
3
)纳米纤维光催化性能,利用静电纺丝技术制备了WO
3
和Ag/WO
3
复合纳米纤维。采用X射线衍射仪(XRD)、扫描电子显微镜(SEM)和紫外-可见分光光度计(UV-Vis),对样品的物相结构、形貌大小和紫外-可见漫反射光谱等进行了表征。在可见光照射下,比较WO
3
和Ag/WO
3
纳米纤维光催化降解亚甲基蓝(MB)的性能,结果表明,在90 min时,Ag/WO
3
复合纤维光催化降解MB效率比WO
3
纤维高1.3倍,从能带结构角度分析了Ag/WO
3
复合纤维光催化效率增强的原理。
In order to study the photocatalytic effect of tungsten oxide(WO
3
) and silver/tungsten oxide(Ag/WO
3
) nanofibers. The WO
3
and Ag/WO
3
nanofibers were fabricated by electrospinning method. The crystal phase
morphology and ultraviolet-visible diffuse reflectance spectroscopy of the samples were characterized by X-ray diffraction(XRD)
scanning electron microscopy(SEM) and UV-Vis spectrophotometer(UV-Vis). The photocatalytic degradation performance on Methyl Blue(MB) with WO
3
and Ag/WO
3
nanofibers was evaluated under UV-Vis light irradiation. The results demonstrate that the photocatalytic degradation efficiency on MB with Ag/WO
3
nanofibers is 1.3 times higher than WO
3
at 90 min. Based on the energy band structure
the principle of photocatalytic efficiency enhancement of Ag/WO
3
composite fibers was analyzed.
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