Preparation of 3,4,9,10-Perylenetetracarboxylic Nanomaterial and Its Sensing Behavior

LI Zhi-ying; ZHOU Xiao-min; HUO Man; ZHANG Hai-rong

doi:10.3788/fgxb20173803.0303

您当前的位置：

首页 >

文章列表页 >

Preparation of 3,4,9,10-Perylenetetracarboxylic Nanomaterial and Its Sensing Behavior

更新时间：2020-08-12

- Preparation of 3,4,9,10-Perylenetetracarboxylic Nanomaterial and Its Sensing Behavior
- Chinese Journal of Luminescence Vol. 38, Issue 3, Pages: 303-307(2017)
- 作者机构：
  
  忻州师范学院化学系, 山西忻州 034000
- 作者简介：
- 基金信息：
  
  Supported by Natural Science Foundation of Shanxi Province(2011011007-1,201601D02024
- DOI：10.3788/fgxb20173803.0303
  CLC： O482.31
- Received：11 September 2016，
  
  Revised：19 November 2016，
  
  Published：05 March 2017
- 稿件说明：
移动端阅览
李志英, 周晓敏, 霍曼等. 3,4,9,10-苝四甲酸二酐纳米材料的制备及其传感行为的研究[J]. 发光学报, 2017,38(3): 303-307

LI Zhi-ying, ZHOU Xiao-min, HUO Man etc. Preparation of 3,4,9,10-Perylenetetracarboxylic Nanomaterial and Its Sensing Behavior[J]. Chinese Journal of Luminescence, 2017,38(3): 303-307
李志英, 周晓敏, 霍曼等. 3,4,9,10-苝四甲酸二酐纳米材料的制备及其传感行为的研究[J]. 发光学报, 2017,38(3): 303-307 DOI： 10.3788/fgxb20173803.0303.

LI Zhi-ying, ZHOU Xiao-min, HUO Man etc. Preparation of 3,4,9,10-Perylenetetracarboxylic Nanomaterial and Its Sensing Behavior[J]. Chinese Journal of Luminescence, 2017,38(3): 303-307 DOI： 10.3788/fgxb20173803.0303.

摘要

以3，4，9，10-苝四甲酸二酐（PTTC）为原料，采用真空气相沉积-分子自组装法制备了有机纳米材料，通过扫描电镜、透射电镜、红外光谱、荧光光谱和差热分析表征所得产物。用吐温20增溶PTTC纳米材料，发现L-赖氨酸对该分散系的荧光具有较强的增敏作用，据此建立了L-赖氨酸的纳米荧光化学传感新方法。体系的荧光变化与赖氨酸浓度呈线性关系，线性范围为7.0010

-4

~5.4010

-7

mol/L，检出限为8.3910

-8

mol/L。进一步研究发现，PTTC纳米结构使赖氨酸的循环伏安图电流差减小，有望据此制作赖氨酸纳米电化学传感器。

Abstract

Organic nanomaterial PTTC was prepared by directly self-assembling in the gas phase with a thermal vacuum evaporation process. The product was characterized by scanning electron microscopy (SEM)

transmission electron microscopy (TEM)

infrared spectrum(IR)、fluorescence spectrum and differential thermal analysis(DTA). The PTTC nanomaterial can be solubilized in the solution of Tween 20

and L-lysine has strong sensitizing effect for the fluorescence of the dispersion system. A nano-fluorescent chemical sensor of L-lysine is built based on the above results. The linear range is 7.0010

-4

-5.4010

-7

mol/L with the detection limit of 8.3910

-8

mol/L. Further study show that the current difference of cyclic voltammogram of L-lysine is reduced by PTTC nanostructure

and it is expected to prepare a nano electrochemical sensor of L-lysine in the future.

关键词

Keywords

references

JI H F, MAJITHIA R, YANG X, et al.. Self-assembly of perylenediimide and naphthalenediimide nanostructures on glass substrates through deposition from the gas phase[J]. J. Am. Chem. Soc., 2008, 130(31):10056-10057.

MCALPINE M C, AHMAD H, WANG D W, et al.. Highly ordered nanowire arrays on plastic substrates for ultrasensitive flexible chemical sensors[J]. Nat. Mater., 2007, 6(5):379-384.

GAO Z Q, AGARWAL A, TRIGG A D, et al.. Silicon nanowire arrays for label-free detection of DNA[J]. Anal. Chem., 2007, 79(9):3291-3297.

FAN H J, WERNER P, ZACHARIAS M. Semiconductor nanowires:from self-organization to patterned growth[J]. Small, 2006, 2(6):700-717.

SAKAMOTO S, PHILIPPE L, BECHELANY M, et al.. Ordered hexagonal array of Au nanodots on Si substrate based on colloidal crystal templating[J]. Nanotechnology, 2008, 19(40):405304.

BECHELANY M, BRODARD P, PHILIPPE L, et al.. Extended domains of organized nanorings of silver grains as surface-enhanced Raman scattering sensors for molecular detection[J]. Nanotechnology, 2009, 20(45):455302.

BECHELANY M, MAEDER X, RIESTERER J, et al.. Sintering mechanisms of organized gold nanoparticles:influence of annealing temperature and atmosphere[J]. Cryst. Growth Des., 2010, 10(2):587-596.

ZHANG H R, XU X H, JI H F. Excitation-wavelength-dependent photoluminescence of a pyromellitic diimide nanowire network[J]. Chem. Commun., 2010, 46(11):1917-1919.

WANG H, XU X H, KOJTARI A, et al.. Triphenylene nano/microwires for sensing nitroaromatics[J]. Phys. Chem., 2011, 115(41):20091-20096.

MOOK W M, NIEDERBERGER C, BECHELANY M, et al.. Compression of freestanding gold nanostructures:from stochastic yield to predictable flow[J]. Nanotechnology, 2010, 21(5):055701.

PARK K H, LEE S, KOH K H, et al.. Advanced nanosphere lithography for the areal-density variation of periodic arrays of vertically aligned carbon nanofibers[J]. J. Appl. Phys., 2005, 97(2):024311-1-4.

ANKER J N, HALL W P, LYANDRES O, et al.. Biosensing with plasmonic nanosensors[J]. Nat. Mater., 2008, 7(6):442-453.

Views

下载量

CSCD

Alert me when the article has been cited

提交

Tools

Publicity Resources

Synthesis and Characterization of 3,3',4,4'-Biphenyl Tetracarboxylic Rare Earth Complexes with Red Fluorescence

Synthesis, Structure and Luminescent Property of 1D Complex [Tb(3,5-pdc)(3,5-Hpdc)(H₂O)(phen)]_n

Synthesis of Novel Blue Light Emitting 9,9'-bianthracene Derivatives and Their Optoelectronic Properties

Synthesis, Characterization and Fluorescence Properties of Complexes of Terbium with Halobenzoic Acid and 2,4,6-tris-(2-pyridyl)-s-triazine

Synthesis, Characterization and Fluorescence Properties of Rare Earth with p-Chloro-benzoic Acid and 2,4,6-Tris-(2-pyridyl)-s-triazine

Related Author

LIN Mei-juan

TANG Qiang

WANG Xiao-ping

Wang Wen

LING Qi-dan

WU Chang-zeng

WANG Hong-sheng

WANG Lei

Related Institution

Fujian Key Laboratory of Polymer Materials, College of Materials Science and Engineering, Fujian Normal University, Fuzhou 350007, China

School of Chemistry and Chemical Engineering, Xuchang University

Xi'an Modern Chemistry Research Institute, Xi'an 710065, China

College of Chemistry and Chemical Engineering, Inner Mongolia University, Huhhot

College of Chemistry and Chemical Engineering, Inner Mongolia University

AI问答

Address：No.3888 Dong Nanhu Road, Changchun, Jilin, China Postal code：130033
Tel：0431-86176862 Email：fgxbt@126.com
Technical support is provided by Beijing Founder electronics co., LTD 吉ICP备11002662号-17 京公网安备11010802024621
It is recommended to read the content of this site in Chrome&IE9+. Please switch to extreme mode in browser 360.
Cookies We use cookies to help provide and enhance our service and tailor content. By continuing, you agree to the use of cookies.

⁰