The Fluorescence Characteristic of Yttrium (Ⅲ)-ciprofloxacin Complex and Its Application

SUN Chun-yan; PING Hong; LI Hong-kun; LI Yong-ji

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The Fluorescence Characteristic of Yttrium (Ⅲ)-ciprofloxacin Complex and Its Application

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- The Fluorescence Characteristic of Yttrium (Ⅲ)-ciprofloxacin Complex and Its Application
- Chinese Journal of Luminescence Vol. 31, Issue 5, Pages: 646-650(2010)
- 作者机构：
  
  吉林大学军需科技学院,吉林长春,130062
- 作者简介：
- 基金信息：
- DOI：
  CLC： O657.3;O482.31
- Received：29 December 2009，
  
  Revised：10 March 2010，
  
  Published Online：21 September 2010，
  
  Published：21 September 2010
- 稿件说明：
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孙春燕, 平红, 李宏坤, 李永吉. 钇(Ⅲ)-环丙沙星配合物的荧光性质及其应用[J]. 发光学报, 2010,31(5): 646-650

SUN Chun-yan, PING Hong, LI Hong-kun, LI Yong-ji. The Fluorescence Characteristic of Yttrium (Ⅲ)-ciprofloxacin Complex and Its Application[J]. 发光学报, 2010,31(5): 646-650
孙春燕, 平红, 李宏坤, 李永吉. 钇(Ⅲ)-环丙沙星配合物的荧光性质及其应用[J]. 发光学报, 2010,31(5): 646-650 DOI：

SUN Chun-yan, PING Hong, LI Hong-kun, LI Yong-ji. The Fluorescence Characteristic of Yttrium (Ⅲ)-ciprofloxacin Complex and Its Application[J]. 发光学报, 2010,31(5): 646-650 DOI：

摘要

研究了稀土钇离子(Y

)与环丙沙星(CPLX)体系的荧光特性

可使体系的荧光强度明显增强

由此建立测定环丙沙星药物的新方法。对CPLX-Y

体系荧光增强的机理进行了初步探讨

并系统研究了CPLX-Y

体系荧光强度的影响因素。在pH=5.5的Tris-HC1缓冲溶液中

浓度为5.010

-5

mol/L时

环丙沙星的浓度与体系的荧光强度呈良好的线性关系

线性范围为1.010

-9

~2.010

-6

mol/L

检出限为3.110

-11

mol/L(S/N=3)。该方法可用于人体尿药浓度和环丙沙星片剂的直接测定。

Abstract

The fluorescence characteristic of the CPLX-Y

complex system was studied in this article. Y

can significantly enhance the fluorescence intensity of the system

and accordingly we established a new sensitive analytical method to determine ciprofloxacin. The influencing factors of the CPLX-Y

fluorescence intensity were thoroughly studied

and the fluorescence enhancement mechanism was preliminary discussed. In the buffer solution of tris-HCl (pH=5.5) with 5.0 10

-5

mol /L of Y

the concentration of CPLX and fluorescence intensity of the system showed good linear relationship. The linear range is 1.010

-9

~2.0 10

-6

mol/L

and the detection limit is 3.110

-11

mol/L(S/N=3). This method can be directly used to determine the CPLX of human urine and CPLX tablet.

关键词

Keywords

references

Mason D J, Power E G, Talsania H, et al. Antibacterial action of ciprofloxacin

. Antimicrob Agents Chemother, 1995, 39 (12):2752-2758.

Zhong Shilong, Wang Xueding, Zhong GuoPing, et al. The pharmaeokinetics and bioequlvalence of ciprofloxac tabletsin in young healthy volunteers

. Guangdong Yaoxue (广东药学), 2003, 13 (3):24-26 (in Chinese).

Fu Lin, Liu Bingyun, Shang Jun. Determination of content in compound enrofloxacin capsules for racing pigeon by ultraviolet spectrophotometry

. Chinese Journal of Veterinary Drug (中国兽药杂志), 2007, (5):31-33 (in Chinese).

Horstkotter C, Jimenez-Lozano E, Barron D, et al. Determination of residues of enrofloxacin and its metabolite ciprofloxacin in chicken muscle by capillary electrophoresis using laser-induced fluorescence detection

. Electrophoresis, 2002, 23 (17):3078-3083.

Schonfeld W, Knoller J, Bremm K D, et al. Determination of ciprofloxacine, norfloxacine, and ofloxacine by high performance liquid chromatography

. Zentral Blatt Fur Mikrobiologie, 1986, 261 (3):338-344.

Liu Yuan, Xie Mengxia, Ding Lan, et al. Simultaneous determination of four luoroquinolones in eggs by high performance liquid chromatography

. Chin. J. Analytical Chemistry (分析化学), 2004, 32 (3):352-355 (in Chinese).

Myers C M, Blumer J L. High-performance liquid chromatography of ciprofloxacin and its metabolites in serum, urine and sputum

. J. Chromatography B:Biomedical Sciences and Applications, 1987, 422 :153-164.

Lin Minling, Liao Rifang, Feng Jiajian, et al. Rapid determination of ciprofloxacin in plasma by LC-ESI-MS/MS

.Strait Pharmaceutical J.(海峡药学), 2009, 21 (5):87-90 (in Chinese).

Liu Xiuli, Hao Yongqing, Si Qin, et al. Determination of ciprofloxacin residues in milk by microbiological method

. Progress in Veterinary Medicine (动物医学进展), 2009, 30 (3):59-62 (in Chinese).

Liu Yongming, Liu Zhenbo, Xu Shuzhou. A molecular imprinting-chemiluminescence method for deternination of ciprofloxacin hydrochloride

. Chin. J. Analysis Laboratory (分析实验室), 2009, 28 (3):47-50 (in Chinese).

Duan J H, Yuan Z H. Development of an indirect competitive ELISA for ciprofloxacin residues in food animal edible tissues

. J. Agric. Food Chem., 2001, 49 (3):1087-1089.

Wang L, Sang L H, Wu Y L, et al. Determination of ciprofloxacin in urine using terbium ion as fluorescent probe

. Spectroscopy and Spectral Analysis (光谱学与光谱分析), 2001, 21 (5):691-693 (in Chinese).

Tong Shanglun, Xiang Guangxiong, Liu Weiping. Study on the determination of ciprofloxacin by the terbium(3+) ion fluorescence probe sensitized by the surfactant

. Spectroscopy and Spectral Analysis (光谱学与光谱分析), 2005, 25 (12):2061-2064 (in Chinese).

Chen Guozhen, Huang Xianzhi, Xu Jingou, et al. Fluorescence Analysis

. Beijing: Science Press, 1990, 61.

Meng Qingyu, Chen Baojiu, Zhao Xiaoxia, et al. Study on UV excitation spectra of Eu3+ or Tb3+ doped Y2O3 nanomate-rials

. Chin. J. Lumin.(发光学报), 2008, 29 (1):107-113 (in Chinese).

Du Liming, Jin Weijun, Dong Chuan, et al. Studies on correlation between protonation and tautomerism and luminescence characteristics of quinolone

. Spectroscopy and Spectral Analysis (光谱学与光谱分析), 2001, 21 (4):518-520 (in Chinese).

Li Huiying. Study on fluorescence enhancement phenomenon of rare earth ions-fluoroquinolone and its analytical application . Shandong: Shandong University, 2006, 17.

Ke Huozhao. Determination and pharmacokinetics research of ciprofloxacin in urine

. Strait Pharmaceutical J.(海峡药学), 2007, 19 (12):106-108 (in Chinese).

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