Synthesis,Characterization and Fluorescence Property of Rare-earth Neodymium with Oxalic Acid and Acrylic Acid

QIU Feng-xian; XU Hong-liang; DA Zu-lin; YANG Dong-ya

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Synthesis,Characterization and Fluorescence Property of Rare-earth Neodymium with Oxalic Acid and Acrylic Acid

更新时间：2020-08-11

- Synthesis,Characterization and Fluorescence Property of Rare-earth Neodymium with Oxalic Acid and Acrylic Acid
- Chinese Journal of Luminescence Vol. 28, Issue 6, Pages: 930-934(2007)
- 作者机构：
  
  江苏大学, 化学化工学院,江苏镇江,212013
- 作者简介：
- 基金信息：
- DOI：
  CLC： O482.31
- Received：10 May 2007，
  
  Revised：12 June 2007，
  
  Published：20 November 2007
- 稿件说明：
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邱凤仙, 徐红良, 笪祖林, 杨冬亚. 稀土钕-丙烯酸-草酸配合物的合成、表征及荧光性能[J]. 发光学报, 2007,28(6): 930-934

QIU Feng-xian, XU Hong-liang, DA Zu-lin, YANG Dong-ya. Synthesis,Characterization and Fluorescence Property of Rare-earth Neodymium with Oxalic Acid and Acrylic Acid[J]. Chinese Journal of Luminescence, 2007,28(6): 930-934
邱凤仙, 徐红良, 笪祖林, 杨冬亚. 稀土钕-丙烯酸-草酸配合物的合成、表征及荧光性能[J]. 发光学报, 2007,28(6): 930-934 DOI：

QIU Feng-xian, XU Hong-liang, DA Zu-lin, YANG Dong-ya. Synthesis,Characterization and Fluorescence Property of Rare-earth Neodymium with Oxalic Acid and Acrylic Acid[J]. Chinese Journal of Luminescence, 2007,28(6): 930-934 DOI：

摘要

合成了钕-草酸-丙烯酸三元固体配合物.利用元素分析、红外光谱(FT-IR)、紫外-可见光谱(UV-Vis)、热重分析(TGA)和荧光光谱等手段研究了配合物的结构和性质.结果表明配合物的组成为[Nd(OOC-COO)(CH

CH-COO)]·3H

热分析结果表明该配合物具有较好的热稳定性.荧光光谱表明配合物都具有较好的荧光特性

且发射谱线很窄

主发射峰为钕离子的

5/2

7/2

9/2

跃迁

表明合成的新型稀土配合物可用作光致发光材料.

Abstract

The novel ternary solid complex of rare earth neodymium(Nd) with oxalic acid(OA) and acroleic acid(AA) was synthesized.The chemical structure and the properties of the complex were characterized by using the element analysis

FT-IR

UV-Vis spectrum

thermal gravimetric analysis (TGA) and fluorescence spectrum.Their composition was determined to be [Nd(OOC-COO)(CH

CH-COO)]·3H

O.The TGA result showed that the complex has excellent thermal stability.The fluorescence spectrum suggested that the innovative complex containing rare-earth ions(Nd

)

with strong characteristic emissions due to the

5/2

7/2

9/2

transition of Nd

ions

is a kind of photoluminescence materials.

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