WANG Xin, GAO Li-juan, YU Shan-sheng, ZHENG Wei-tao, XU Wei, GUO Wei, YANG Kai-yu. Kinetic Scaling of Iron Nitride Thin Films Deposited by DC Magnetron Sputtering[J]. Chinese Journal of Luminescence, 2003,24(4): 431-434
WANG Xin, GAO Li-juan, YU Shan-sheng, ZHENG Wei-tao, XU Wei, GUO Wei, YANG Kai-yu. Kinetic Scaling of Iron Nitride Thin Films Deposited by DC Magnetron Sputtering[J]. Chinese Journal of Luminescence, 2003,24(4): 431-434DOI:
Kinetic Scaling of Iron Nitride Thin Films Deposited by DC Magnetron Sputtering
Iron nitride films have received attention for many years. Initially
they have been studied because of their ability to improve surface hardness and wear resistance. Recently
the FeN thin films have been widely investigated since they show a variety of structures and magnetic properties. All nitrides with the composition of Fe
x
N(
x
≥3) are ferromagnetic and stable at room temperature. In particular
α″-Fe
16
N
2
phase is the most important compound and can be a possible candidate for high density magnetic recording media owing to its very high magnetic moment even higher than that of pure iron. However
up to now
little research has been done to investigate the dynamical scaling behavior of iron nitride films sputtered on glass to determine its universality class although dynamic scaling may be a useful method for understanding the formation of structure of the thin films. There are three types of growth morphologies:layer by layer growth
unstable growth
and self affine surface. Solid films grown under far from equilibrium conditions are predicted to have self affine surfaces
and the roughness can be characterized by appealing to a dynamic form. Moreover
the KPZ equation has proven to be a universal equation for real surface growth phenomena only on the basis of computer simulations. There is nearly no unambiguous experimental demonstration of KPZ growth. In this study
we deposited iron nitride thin films by DC magnetron sputtering at mixed Ar/N
2
discharges(N
2
fraction of 5%
10%
30%
50%
respectively) and different times(160
30
20
10
5min) in order to study their kinetic scaling behavior. The composition of the films was analyzed using X-ray photoelectron spectroscopy experiment (XPS). The layer phases and surface morphology of the films were characterized using grazing incidence X-ray scattering and X-ray diffraction as well as atomic force microscopy. For the film grown at N
2
fraction of 30% and 50%
the phase of FeN appears
if the N
2
fraction is 10%
the phase of ε Fe
3
N is formed
while the phase of FeN
0.056
occurs for the film deposited at N
2
fraction of 5%. The surface of the films deposited at N
2
fraction of 5% showed a self affine character. The values of roughness exponent α≈0.65 and growth exponent β≈0.53±0.02 are in agreement with the improvised KPZ exponents based on Kolmogorov’s energy cascade concept.
DC magnetron-sputtered VO2 thin films: towards high-performance near-infrared photodetectors
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YANG Qi
ZENG Ming
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YANG Liu
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Related Institution
Hubei Key Laboratory of Micro-Nanoelectronic Materials and Devices,Institute of Industrial Technology at Qianjiang,School of Microelectronics,Hubei University