THE DETERMINATION OF CHLOROGENIC ACID BY CHEMILUMINESCENCE ANALYSIS

He Caixia; Lu Minggang; Cui Hua; Zhao Guiwen

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THE DETERMINATION OF CHLOROGENIC ACID BY CHEMILUMINESCENCE ANALYSIS

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- THE DETERMINATION OF CHLOROGENIC ACID BY CHEMILUMINESCENCE ANALYSIS
- Chinese Journal of Luminescence Vol. 18, Issue 1, Pages: 65-70(1997)
- 作者机构：
  
  中国科学技术大学应用化学系, 合肥230026
- 作者简介：
- 基金信息：
- DOI：
  CLC：
- Received：13 June 1996，
  
  Published：28 February 1997
- 稿件说明：
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贺彩霞, 陆明刚, 崔华, 赵贵文. 化学发光分析法测定绿原酸[J]. 发光学报, 1997,18(1): 65-70

He Caixia, Lu Minggang, Cui Hua, Zhao Guiwen. THE DETERMINATION OF CHLOROGENIC ACID BY CHEMILUMINESCENCE ANALYSIS[J]. Chinese Journal of Luminescence, 1997,18(1): 65-70
贺彩霞, 陆明刚, 崔华, 赵贵文. 化学发光分析法测定绿原酸[J]. 发光学报, 1997,18(1): 65-70 DOI：

He Caixia, Lu Minggang, Cui Hua, Zhao Guiwen. THE DETERMINATION OF CHLOROGENIC ACID BY CHEMILUMINESCENCE ANALYSIS[J]. Chinese Journal of Luminescence, 1997,18(1): 65-70 DOI：

摘要

本文基于碱性介质中绿原酸对鲁米诺-铁氰化钾化学发光体系的抑制作用

首次建立了绿原酸的化学发光分析法

并探讨了其作用机理。方便简便、迅速、重复性好、灵敏度高。采用该法可测定1.0×10

-8

g/ml～1.0×10

-5

g/ml范围内的绿原酸

其检出限达到5.2×10

-9

g/ml

回收率为104%.

Abstract

A new chemiluminescence method has been developed for the determination of chlorogenic acid by using the inhibition of chlorogenic acid on the chemiluminescence reaction of Luminol potassium ferricyanide. The method is simple

convenient and sensitive with a detection limit of 5.2×10

-9

g/ml. It is effective to determine chlorogenic acid in the range of 1×10

-8

g/ml～1×10

-5

g/ml. The variation coefficient of eleven determinations for 5×10

-7

g/ml chlorogenic acid is 1.7%

and recovery is 104%. Furthermore

the inhibition mechanism was discussed in this paper.

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